Identify the two amino acids created by these dipeptides, andlabel all of the peaks in the 'H NMR and C NMR.
Synthesis and Identification of a Dipeptide PER BocHN R OH + EDCI-HCI = R₁ OCH3 EDCI-HCI Et3N Boc = t-butoxycarbonyl = 1-ethyl-3-(3'-dimethylaminopropyl) carbodiimide hydrochloride BocHN. to St N=C=N R O R' N O To N-H OCH3
X: parts per Million : 1H 3.746 2.176 1.938 1.444 1.409 1.394 0.956 0.944 0.932 7.0 50 4.0 abundance 0 1.0 0.24 1.00 0.37 1.04 0.83 1.06 2.0 1.90 2.10 3.18 3.0 4.0 6.44 5.0 6.0 7.0 12.54 8.0
170.0 160.0 150.0 140.0 130.0 X: parts per Million: 13C 120.0 110.0 100.0 90.0 80.0 80777 70.0 60.0 50.0 40.0 30.0 20.0
Identify the two amino acids created by these dipeptides, and label all of the peaks in the 'H NMR and C NMR.
-
- Site Admin
- Posts: 899603
- Joined: Mon Aug 02, 2021 8:13 am