Bu Br 1) 1.05 nBuLi 30 min -78 C 30 min RT 2) 0.25 Cl₂PCH₂CH₂PC12 -78 to RT 24h Ether 3) H₂O tBu tBu JG4 1 1 /opt/topsp

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Bu Br 1 1 05 Nbuli 30 Min 78 C 30 Min Rt 2 0 25 Cl Pch Ch Pc12 78 To Rt 24h Ether 3 H O Tbu Tbu Jg4 1 1 Opt Topsp 1 (33.18 KiB) Viewed 40 times

Bu Br 1) 1.05 nBuLi 30 min -78 C 30 min RT 2) 0.25 Cl₂PCH₂CH₂PC12 -78 to RT 24h Ether 3) H₂O tBu tBu
JG4 1 1 /opt/topspin4.1.4/NMR Mouse Sensitivity: 1.0 -3.19 ppm / -1914.89 Hz Sum 15.2700 DEFINE REGION MODE Define: Drag using left mouse button Return: Left-click highlighted icon 15 10 ft. 1.0000 0.5705 5 1.1618 -0.9535 1.7457 7.7345 1.3486 0.7553 [ppm] 12 [rel] 10 8 9 4 7 0 7
JG4 2 1 /opt/topspin4.1.4/NMR Mouse Sensitivity: 1.0 -244.7 ppm / -59445.8 Hz Sum= 1.2605 DEFINE REGION MODE Define: Drag using left mouse button Return: Left-click highlighted icon 100 0000'T 0.2605 100 200 [ppm] ▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬ [rel] 3 2