(45 points) Solve the following compound from the given spectra.
Show what information you have taken from each spectrum. In
correlation spectroscopy show the connectivity.
\\Please, interpret all 7 provided spectra to get useful
information about the compound. The connectivity in the correlation
spectroscopy is also compulsory. Provide correct, full, and
understandable answers, otherwise do not send obviously incorrect
and incomplete answers.
MASS 1097 100 % of Base Peak 1247 50 43 537 817 40 50 60 70 80 m/z 90 100 110 120 IR 100 IMMAN 50 % Transmittance IT -31241 -29241 -16741 --15201 - 12964 9701 - -802 4000 3000 1000 2000 Wavenumber (cm-1)
'H NMR 600 MHz بال זייןייז יד 4230 4220 Hz ۲۲۲۲۲۲۲ 3670 3660 Hz 1420 1410 HZ 5.0 4.5 4.0 3.5 3.0 2.5 ppm 7.0 6.5 6.0 5.5 13C/DEPT NMR 150.9 MHz 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 ppm
7.5 7.0 6.5 6.0 55 50 4.5 4.0 3.5 3.0 25 2.0 wwwww Ppm Ppm COSY 600 MHZ F1 F2 HMQC 600 MHZ ppm 20- 20 40- 40 60 60 80 FI 80 100- 100 120- 120 140- 140 PTT 7.5 7.0 6.5 6.0 55 50 4.5 4.0 35 3.0 25 2.0 F2 ppm
HMBC 600 MHz 72 7.0 6.8 6.6 6.4 6.2 24 23 ppm Ppm افلفليطها - 20- 20 - 30- 30 40 40 50- 50 60- 60 70- 70 80 80 F1 90- 90 100- 100 110- 110 120- -120 130 130 140- 140 150 150 160- 160 170- -170 180- 180 72 7.0 6.5 6.6 6.4 62 2.4 2.3 Ppm ppm F2
(45 points) Solve the following compound from the given spectra. Show what information you have taken from each spectrum
-
- Site Admin
- Posts: 899603
- Joined: Mon Aug 02, 2021 8:13 am