Unknown 39 Component B EI MS 105 100 miz Relative Intensity 1 1 4 26 27 28 37 77 38 39 41 42 43 44 49 50 1 2 5 S 7 7 1 2

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Unknown 39 Component B Ei Ms 105 100 Miz Relative Intensity 1 1 4 26 27 28 37 77 38 39 41 42 43 44 49 50 1 2 5 S 7 7 1 2 1 (55.87 KiB) Viewed 62 times

Unknown 39 Component B EI MS 105 100 miz Relative Intensity 1 1 4 26 27 28 37 77 38 39 41 42 43 44 49 50 1 2 5 S 7 7 1 2 18 1 2 17 38 4 1 1 2 3 3 1 51 52 53 61 62 63 64 65 73 74 50 2 51 75 76 77 78 89 91 120 1 5 3 5 87 8 1 1 2 2 100 7 30 2 105 106 120 43 50 121 78 74 76 27 26 28 6365 39 38 37 42 44 + 40 52 49 53 50 73 79 86 8991 0 98 103 100 20 30 60 70 80 90 110 하 120 130 Elemental Analysis: C, 79.97; H, 6.71; 0, 13.32%.

Unknown 39 Component B FTIR (ATR) 100 10 -1819 S1302 S-1102-107 -1001 S731 85 21428 1582 1180 -1024 4500 BVY -954 s B། ༦། ། ཅ ཆ % | | | | | | %Transmittance cm-1 %T cm-1 %T 586 17 1263 18 617 90 1302 85 688 21 1358 45 731 87 1428 83 757 27 1449 70 848 96 1582 79 927 86 1599 68 95462 1681 21 1001 91 1819 98 1024 78 1911 1911 98 1078 84 1975 99 1102 93 3005 96 1160 91 3063 95 1180 81 3354 99 35 15 10 5 4000 О до00 3000 2000 1000 Wavenumber (cm-1)

Unknown 39 Component B 13C NMR 75 MHz CDC13 - 137.1 (128.3 DEPT135 75 MHz CDCI 200 180 140 30 160 ppm 20 wwwwwwwwwwwwwww wwwth Win wwwwwwwwww 220 210 200 190 180 170 160 150 140 130 120 100 90 80 70 60 50 40 30 20 10 0 -10 110 ppm

Unknown 39 Component B NNNNN 1H NMR 300 MHz CDC13 9 whit 8.00 7.95 7.55 7.50 7.45 7.90 7.60 ppm H2O 10.5 10.0 9.5 9.0 8.5 8.0 7.5 7.0 6.5 6.0 5.5 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 -0.5 5.0 ppm