- Ms Ir Nmr Here Are The Report Assigment 1 (20.07 KiB) Viewed 24 times
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100 Thu Apr 28 16 01 11 2022 (GMT-0400) 98 96 94 26 90 88 els then 98 2836.12 2360.18 84 % Transmittance 300432 82 1175.10 80 823.40 78 76 1029 83 74 72 3421.01 70 3346.46 68 1228.62 1503 86 66 3500 3000 1500 2500 2000 Wavenumbers (cm-1) 1000
#16 Salem, 1H, Unknown wels BRUKER tise INSTRUM PROBUD PUL PROG cock Current Data Parameters NAME Salen_Unkn16_11 EXPND 25 PROCNO F2 - Acquisition Parameters Date 20220429 14.36 spect 2108628_1066 5930 TD SOLVER 65536 NS DS 2 SWI HS FIDRES 0.244532 4.0894465 sec RG DW 64 62.400 user DE 17.09 wec TE 296.6 X 1.00000000 sec TDO STO 400.1324708 MI: NUCI IN PO Pi 14.00 sec 12.55799961 W F2 - Processing parameters 65536 400.1300000 t EM ssa 0.30 H 1.00 4.67 usec 385383 73203238285 1.77 1.80 2.50 3.00 10 9 8 7 6 5 4 3 3 N 1 ppm
Salem, Unknown #16, 130 55.76 BRUKER EXPO Dace PROBND CON VIORES 6.50 sec Current Data Parameters NAME Salen_tinkn16_13C 26 PROCHO 12 - Acquisition Parameters Tine 20220429 14.50 INSTRUM spect 2108618_1066 PULPROG TD mag30 65536 SOLVENT 32 DS SMN 24038.461 a AQ 0.733596 Ha 1.3631488 sec RG 161 DW 20.800 sec DE TE 297.4 K DI 2.00000000 sec 031 0.03000000 sec TDO 1 100.6228298 MHz 20 136 3.33 used 2.1 $3.53799820 W 10.00 sec 400.1316005 MHZ 1H waitas PING 12.55799961 W P2 0.30386999 W PLAI 0.15285000 W F2 - Processing parameters SI 32768 SY 100.6127685 MHz WOW EN ppm ssa o 1.00 Hz СВ 0 PC 1.40 STOR NOCE PLAZ CPOPRO 12 PCPD 90.00 sec 200 180 160 140 120 100 80 60 40 20 0
Enter the molecular formula chosen from the m/z of the molecular ion. In the MS Assignments table, enter any MS fragments that may have been helpful. There may be none. (You are only expected to enter the molecular ion, but if you can enter correct fragments, it will help recover lost points elsewhere in the report. No scores will be given over the maximum worth of the report.) Enter the diagnostic IR peaks and their assignments in the IR table. You will not be able to assign every peak. In the HNMR table enter the data requested for each absorption. You should be able to make some type of assignment for each one. Finally, enter assignments for the C NMR peaks. Enter the data and assignments in the manner that was requested for Quiz 3. Molecular formula MS Assignments mizol peak Assignment IR Assignments Absorption (cm) Assignment
IR Assignments Aaron Augreat 'H NMR Assignments CSC We won "C NMR Assignments Chemtraigment Structure of the second compound assigned with your unknown In this part, you will assume that your unknown and the second compound are both dissolved in diethy! ether. They can be separated by extractions using a separatory funnel (In some cases, it won't be perfect but will be OK here.) Draw the structure of each compound in the top box provided. Then, assume that this ether later was extracted first with aq. 1 M HCI. Then assume the ether layer was extracted with aq. 1 M NaOH. Indicate whether the compounds will stay in the ether layer, be extracted in the aq, 1 M HCl extract or the aq. 1 M NaOH extract by drawing their structures in the appropriate box where it will be dissolved. Unknown Compound Dich in Delhi
**C NMR Assignments Che Art Structure of the second compound assigned with your unknown In this part, you will assume that your unknown and the second compound are both dissolved in diethyl ether. They can be separated by extractions using a separatory funnel. (In some cases, it won't be perfect but will be OK here.) Draw the structure of each compound in the top box provided. Then, assume that this ether later was extracted first with aq. 1 M HCL Then assume the ether layer was extracted with aq. 1 M NaOH. Indicate whether the compounds will stay in the ether layer, be extracted in the aq. 1 M HCl extract or the aq. 1 M NaOH extract by drawing their structures in the appropriate box where it will be dissolved. Lindrom Assigned Comune Dissolved in Dietyl Ether Eyerere Aqyer er extraction with a TM мион