what is the peak area that belongs to morphine in each of the
following GC-MS images. Based on what should I analyze which ion is
codeine and which ion is morphie?
Sample : M5C1 Misc : ALS Vial : 26 Sample Multiplier: 1 Integration Parameters: Toxt.p Integrator: RTE Filtering: 5 Smoothing: ON Sampling : 1 Min Area: 1111 Area counts Max Peaks: 3 Start Thrs: 0.2 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Tangent else baseline drop > Peak separation: 0 : C:\msdchem\1\methods\default.m Method Title : Signal : EIC Ion 327.00 (326.70 to 327.70): M5C1. D\data.ms Deak R.T. first max last PK peak corr. area corr. % max. % of total # min scan scan scan TY height 1 5.926 165 169 175 rBB 7880 12887 86.70% 34.188% 2 6.525 212 219 rBB3 7119 201 646 648 14864 100.00% 39.433% 9943 66.89% 26.378% 3 12.596 652 rBB 9430 Sum of corrected areas: 37694 Signal : EIC Ion 330.00 (329.70 to 330.70): M5C1.D\data.ms corr. Deak R.T. first max last PK peak scan scan scan TY height corr. area % of total # min % max. 12.582 645 647 658 rBB 7309 11541 100.00% 100.000% Sum of corrected areas: 11541 M5C1.D\data.ms : EIC Ion 341.00 (340.70 to 341.70): corr. corr. area % max. 17856 84.26% 9762 46.06% 21192 100.00% 48810 1 Signal beak R.T. first max last PK peak scan scan scan TY height 13353 128 130 132 RBB 201 212 224 rBB 4375 610 614 619 rBB2 20550 Sum of corrected areas: # min 1 5.383 2 6.525 3 12.122 HNM % of total 36.583 % 20.000% 43.417%
Data File: M5C2.D Acq On : 16 Apr 19 04:51 am Operator : Sample : M5C2 Misc : ALS Vial : 27 Sample Multiplier: 1 Integration Parameters: TOXt.p Integrator: RTE Filtering: 5 Smoothing: ON : 1 Sampling Min Area: 1311 Area counts Max Peaks: 5 Start Thrs: 0.2 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Tangent else baseline drop > Peak separation: 0 : C:\msdchem\1\methods\default.m Method Title : Signal : EIC Ion 327.00 (326.70 to 327.70): M5C2.D\data.ms peak R.T. first max last PK peak corr. corr. area # min scan scan scan TY height max. total ‒‒‒‒- -‒‒‒‒‒‒‒‒ ------- ‒‒‒‒‒‒- 1 4.952 92 99 103 BB 1407 5643 30.59% 14.518€ 2 5.383 127 130 133 BB 2970 12.162 € 3 5.940 166 170 175 BB2 3508 4727 25.62% 5479 29.70 € 18449 100.00% 14.096% 4 6.525 200 212 218 xBB3 8931 47.466% 5 12.596 648 654 BB 3846 4570 24.77% 11.758% Sum of corrected areas: 38868 Signal : EIC Ion 330.00 (329.70 to 330.70): M5C2.D\data.ms peak R.T. first max last PK peak # min scan scan scan TY height corr. area corr. max. & of total --- ‒‒‒‒- ‒‒‒‒ ----- ---- --- 1 12.582 645 647 658 BB 2067 3761 100.00% 100.000 € Sum of corrected areas: 3761 M5C2.D\data.ms Signal EIC Ion 341.00 (340.70 to 341.70): corr. corr. peak R.T. first max last PK peak # min scan scan scan TY height % of total area & max. ---
Sample : M5C3 Misc : ALS Vial : 28 Sample Multiplier: 1 Integration Parameters: TOXt.p Integrator: RTE Smoothing: ON Sampling : 1 Filtering: 5 Min Area: 1311 Area counts Start Thrs: 0.2 Max Peaks: 1 Stop Thrs 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Tangent else baseline drop > Peak separation: 0 : C:\msdchem\1\methods\default.m Method Title : Signal : EIC Ion 327.00 (326.70 to 327.70): M5C3.D\data.ms R.T. first max last PK peak scan scan scan TY corr. area corr. & max. & of total min height ----- ------ ‒‒‒‒‒‒ 12.596 645 648 660 BB2 28178 31023 100.00% 100.000% Sum of corrected areas: 31023 EIC Ion 330.00 (329.70 to 330.70): M5C3.D\data.ms R.T. first max last PK peak corr. corn. & of min scan scan scan TY height area max. total ‒‒‒‒‒ ‒‒‒‒‒ ‒‒‒‒‒‒‒ ‒‒‒‒‒‒‒ ‒‒‒‒‒‒ ‒‒‒‒ 1 12.582 643 647 661 BB2 8424 12364 100.00% 100.000* Sum of corrected areas: 12364 Signal : EIC Ion 341.00 (340.70 to 341.70): M5C3.D\data.ms peak R.T. first max last PK peak corr. area corr. & max. & of total # min scan scan scan TY height ----- ===== ---- ---- --- 12.122 611 614 619 BB2 50378 54660 100.00% 100.000% Sum of corrected areas: 54660 M5C3.D\data.ms : EIC Ion 344.00 (343.70 to 344.70): corr. corr. area % of total * max. 22811 100.00% 100.000% 22811 peak # 1 Signal peak # 1 Signal peak R.T. first max last PK peak scan scan scan TY height # min ---- 12.108 609 613 623 BB2 20096 1 Sum of corrected areas:
Sample : M5C4 Misc : ALS Vial : 29 Sample Multiplier: 1 Integration Parameters: TOXt.p Integrator: RTE Smoothing: ON Filtering: 5 Sampling : 1 Min Area: 1311 Area counts Start Thre: 0.2 Max Peaks: 1 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Tangent else baseline drop > Peak separation: 0 : C:\msdchem\1\methods\default.m Method Title : Signal : EIC Ion 327.00 (326.70 to 327.70): M5C4.D\data.ms corr. peak R.T. first max last PK peak # min corr. area & of total scan scan scan TY height € max. 1 12.596 645 648 660 BB2 63870 68936 100.00% 100.000€ Sum of corrected areas: 68936 330.70): M5C4. D\data.ms Signal : EIC Ion 330.00 (329.70 to corr. peak R.T. # min first max last PK peak scan scan scan TY height corr. area & of total € max. ---- ‒‒‒‒‒‒ 1 12.582 643 647 658 BB2 10970 13472 100.00% 100.000€ Sum of corrected areas: 13472 Signal : EIC Ion 341.00 (340.70 to 341.70): M5C4. D\data.ms peak R.T. first max last PK peak corr. area scan scan scan TY height corr. & max. # min total --- ‒‒‒‒ ---- --- 611 614 619 xBB2 102994 122458 100.00% 100.000 € Sum of corrected areas: 122458 M5C4.D\data.ms : EIC Ion 344.00 (343.70 to 344.70): corr. corr. area max. total ‒‒‒‒‒‒‒ ‒‒‒‒‒‒ ‒‒‒‒ 27175 100.00% 100.000 € 27175
Sample : MST10 Misc : ALS Vial : 31 Sample Multiplier: 1 Integration Parameters: TOXt.p Integrator: RTE Smoothing: ON Filtering: 5 Sampling : 1 Min Area: 1311 Area counts Start Thrs: 0.2 Max Peaks: 1 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Tangent else baseline drop Peak separation: 0 : C:\msdchem\1\methods\default.m Method Title : Signal : EIC Ion 327.00 (326.70 to 327.70): M5T10.D\data.ms peak R.T. first max last PK peak corr. corr. & of # min scan scan scan TY height area max. total ‒‒‒‒‒ ‒‒‒‒ ---- 1 12.596 645 648 654 BB2 52235 56010 100.00% 100.000% Sum of corrected areas: 56010 Signal : EIC Ion 330.00 (329.70 to 330.70): M5T10.D\data.ms peak R.T. first max last PK peak corr. corr. & of # min scan scan scan TY height area max. total --- ‒‒‒‒‒ ‒‒‒‒‒‒‒ ‒‒‒‒‒‒ ‒‒‒‒‒‒‒ 1 643 647 657 BB2 9059 10506 100.00% 100.000* Sum of corrected areas: 10506 M5T10.D\data.ms Signal EIC Ion 341.00 (340.70 to 341.70): corr. corr. & of peak R.T. first max last PK peak # scan scan scan TY height min area max. total --- ‒‒‒‒‒ ---- ‒‒‒‒‒‒‒ ----- ‒‒‒‒‒ 1 12.122 609 614 619 BB2 76035 104607 100.00% 100.000% Sum of corrected areas: 104607 Signal : EIC Ion 344.00 (343.70 to 344.70): M5T10.D\data.ms peak R.T. first max last PK peak corr. area corr. & max. # min scan scan scan TY height total --- ‒‒‒‒‒‒‒ 12.108 611 613 618 BB2 22234 22323 100.00% 100.000% Sum of corrected areas: 22323 1 12.582
Sample Name: M5C1 Misc Info : Vial Number: 26 Abundance Ion 327.00 (326.70 to 327.70): M5C1.D\data.ms 12.596 8000 6.525 6000 4000 2000 tr of Time--> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Abundance Ion 330.00 (329.70 to 330.70): M5C1.D\data.ms 12.582 7000 6000 5000 4000 3000 2000 1000 0...……… od .………………. ……………………… ----------- Time-->> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Ion 341.00 (340.70 to 341.70): M5C1.Didata.ms Abundance 12.122 20000 5.383 15000 10000 5000 6.525 0 Time-->> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Abundance Ion 344.00 (343.70 to 344.70): M5C1.D\data.ms 12.108 20000 15000 10000 5000 of 0+…………………………………… *|*|*|*|||||||||||||||||| ™T 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Time--> 5.926 سلسل
Sample Name: M5C2 Misc Info : Vial Number: 27 Abundance 8000 6000 4000 2000 Ion 327.00 (326.70 to 327.70): M5C2.D\data.ms 12.596 4.952 OFF ----…….…………………. **********…………….. 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Ion 330.00 (329.70 to 330.70): M5C2.D\data.ms 12.582 of Time--> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Abundance Ion 341.00 (340.70 to 341.70): M5C2.D\data.ms 5.383 25000 20000 15000 12.122 10000 4.910 6.525 5000 INV of 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Ion 344.00 (343.70 to 344.70): M5C2.D\data.ms 12.108 5.383 of 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Time--> Abundance 2000 1500 1000 500 Time--> Abundance 8000 6000 4000 2000 Time--> 5.940 5.383 6.$25 بالسر 5.592
Sample Name: M5C3 Misc Info Vial Number: 28 Abundance 25000 Ion 327.00 (326.70 to 327.70): M5C3.D\data.ms 12.596 15000 10000 5000 omr Time--> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Abundance Ion 330.00 (329.70 to 330.70): M5C3.D\data.ms 12.582 8000 6000 4000 -^ Ot.…..…….……………..…… .......…....per pepp Time-->> Abundance 50000 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Ion 341.00 (340.70 to 341.70): M5C3.D\data.ms 12.122 40000 30000 20000 10000 of wwwwwww T Time--> Abundance 200001 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Ion 344.00 (343.70 to 344.70): M5C3.D\data.ms 12.108 15000 10000 5000 of www 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 200 10 50 11001 sol cool......……….. 20000 2000 Time-->
Sample Name: M5C4 : Misc Info Vial Number: 29 Abundance Ion 327.00 (326.70 to 327.70): M5C4.D\data.ms 12.596 60000 50000 40000 30000 20000 10000 P AAST Time--> Abundance 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Ion 330.00 (329.70 to 330.70): M5C4.D\data.ms 12.582 10000 8000 6000 4000 2000 wwwwwwwwww.p Time-->> Abundance 100000 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Ion 341.00 (340.70 to 341.70): M5C4.D\data.ms 12.123 80000 60000 40000 20000 ofertery *************** 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Ion 344.00 (343.70 to 344.70): M5C4.D\data.ms 12.109 of T 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Time--> Abundance 25000 20000 15000 10000 5000 Time-->
Sample Name: M5T10 Misc Info : Vial Number: 31 Ion 327.00 (326.70 to 327.70): M5T10.D\data.ms Abundance 50000 12.596 40000 30000 20000 10000 TIPPTATT www Time-->> Abundance 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Ion 330.00 (329.70 to 330.70): M5T10.D\data.ms 12.582 8000 6000 4000 2000 of 0+...………...……….……….. www. TT Time--> Abundance 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Ion 341.00 (340.70 to 341.70): M5T10.D\data.ms 12.122 70000 60000 50000 40000 30000 20000 10000 o..……..….........……...www. Time--> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Abundance Ion 344.00 (343.70 to 344.70): M5T10.D\data.ms 12.108 20000 15000 10000 5000 of ™T 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 Time-->