4. Based on the amount of water you used during the
recrystallizalion (35 ml of water used),
estimate the amount of salicylic acid that was lost as a result of
being
dissolved in the filtrate. Assume that the recrystallization
solution was
cooled to 10°C; the solubility of salicylic acid at that
temperature is
0.14 g per 100 mL of water.
5. Describe and explain the possible effect on your results of the
follow-
ing experimental errors or variations. (a) You added only enough 3
M
H,SO, to bring the pH down to 4. (b) Your reaction mixture had an
oily
layer on top when you added the 3 M sulfuric acid. (c) Because of
a
label-reading error by a lab assistant, the bottle labeled
"salicylic acid
from benzene" actually contained acetylsalicylic acid
(aspirin).
4. Based on the amount of water you used during the recrystallizalion (35 ml of water used), estimate the amount of sali
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4. Based on the amount of water you used during the recrystallizalion (35 ml of water used), estimate the amount of sali
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