I just want you to rephrase this in fluent text in the past tense. Dry list: all the glassware must before use be drying

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answerhappygod
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I just want you to rephrase this in fluent text in the past tense. Dry list: all the glassware must before use be drying

Post by answerhappygod »

I just want you to rephrase this in fluent text in the past
tense.
Dry list: all the glassware must before use be drying in
a hot oven over 120 grader. The glassware and reactants are:
100ml three neck flask, 25ml additional funnel, separatory funnel,
additional funnel, rounded bottom flask, guard tube, magnet,
magnesium and reflux condenser parts.
Set up a 100ml three neck flask with 25ml additional
funnel. Then take a protective tube of calcium chloride to protect
the reflux condenser and a magnetic stirrer bar.

in a the three neck flask add 0,4 g magnesium and
15 ml dried diethyl
ether

In the additional funnel add 1,2g benzyl bromide and 15
ml of dry diethyl ether.

Start the stirrer and wait until formation of the
grignard reagent starts.

while stirring add dropwise the remaining bromide
solution to the formation every 15 min then after adding the whole
bromide solution stir the solution in 10 min

add 1 ml of cyclohexanone + 10ml diethyl ether in
the additional funnel and let it drip on the Grignard reagent into
a three neck round bottom flask

sir the mixture for a 15 minutes

Add 10 mL water to the solution then let it drip to the
grignard solution

add 10 mL 5% diluted HCl in additional funnel and let it
drip to the solution

pour off the mixture from any remaining magnesium into
the separatory funnel, then separate the ether layer (org.
layer).

wash the org layer (diethyl layer) with 10ml 5% sodium
hydroxide solution and
separate the org layer again.

dry it with magnesium sulfate

glass wool filter the dried solution

Do TLC-test

place the solution in a rotary evaporator

run IR- and NMR-spectra.
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