SECTION C-EXPERIMENTAL CHEMISTRY [12] AFDELING C-EKSPERIMENTELE CHEMIE [12] You are required to perform one of the synth
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SECTION C-EXPERIMENTAL CHEMISTRY [12] AFDELING C-EKSPERIMENTELE CHEMIE [12] You are required to perform one of the synth
SECTION C-EXPERIMENTAL CHEMISTRY [12] AFDELING C-EKSPERIMENTELE CHEMIE [12] You are required to perform one of the synthetic steps to make Van u word verwag om een van die sintetiese stappe te doen om illudinine, specifically the formation of compound 12 shown in the illudinien te maak, spesifiek die vorming van verbinding 12 wat in scheme below. Please do the following: die skema hieronder getoon word. Doen asseblief die volgende: • Complete the table of calculations. [4] Voltooi die tabel van berekeninge. [4] Calculate the theoretical yield (mass) of the product [2] Bereken die teoretiese opbrengs (massa) van die produk. [2] Suggest a procedure to synthesise the required product, and Stel 'n prosedure voor om die vereiste produk te sintetiseer en isolate it after the reaction. No purification step is required, but dit na die reaksie te isoleer. Geen suiwering stap word benodig you should use a work-up procedure to remove the acidic nie, maar jy moet 'n opwerkingsprosedure gebruik om die TsOH catalyst. Please also give approximate volumes of all suur-TSOH-katalisator te verwyder. Gee ook ongeveer volumes liquids used in your proposed procedure. [6] van alle vloeistowwe wat in u voorgestelde prosedure gebruik word [6] HO OME Оме TsOH (cat.) Me 22 Me Me Me PhCH3 reflux, 10 min CO2Me CO2Me 12 11 Reagent / Reagens Formula / Formule Molar mass/ Molêre massa Mass / Massa mmol Equivalents/ Ekwivalente Compound 11 2.00 g TsOH G,H,O,5 Product/ Produk Formula / Formule Molar mass/ Molêre massa Theoretical yield / Teoretiese opbrengs Compound 12 Synthetic procedure / Sintetiese prosedure
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