- Transmittance 100 95 90 85 80 75 70 65 60 55 50 45 40 Transmittance 3328 1 4000 3228 1 0 H Stretch 2853 1 (403.06 KiB) Viewed 34 times
through Chapman-Stevens oxidation reaction
→ Chapman-Stevens oxidation - done by simply adding the
acetic acid and sodium hypochlorite, which is also known as
hypochlorous acid to cyclohexanol and then separating the final
product from the by-products
QUESTION: Explain that cyclohexanone was
successfully synthesized based on IR. Please provide an explanation
if possible. Thanks!
% Transmittance 100 95 90- 85- 80- 75- 70- 65 60- 55- 50- 45- 40- % Transmittance 3328.1 4000 3228.1 → 0-H stretch 2853.1-2927.4 → C-H stretch 100 95- 90- 85- 80- 75- 70- 65- 60- 55 50- 45- 40- 35- 30- cyclohexanol reference 3500 3000 2500 2000 1500 Wavenumbers (cm-1) Figure 1: IR spectrum of reactant cyclohexanol 2853.1 4000 3500 2861.31 - 2932.90 → C-H stretch 1705.15 → C=O stretch 2927.4 2861.31 2932.90 reaction product 3000 2500 2000 Wavenumbers (cm-1) Figure 2: IR Spectrum of product 1703.5 1705.15 1500 1449.7 1138.4 1236.5 1255.2 1296.4 1345.7 1362.3 1449.03 1173.0 1338.13 1422 10.71 1064.2 966.6 1024.6 1000 1221 14 788.5 889.1 pro 1071.76907.94 844.0 1118.25 1000 1017 82863.79 74