Answer Happy

Posted: **Mon Jul 11, 2022 2:03 pm**

: Given The Accompanying Gc Ms Data Pgs 8 10 26 Is The Crude Product A B Ready For Re Distillation A Or Should It 1 (14.98 KiB) Viewed 36 times

: Given The Accompanying Gc Ms Data Pgs 8 10 26 Is The Crude Product A B Ready For Re Distillation A Or Should It 2 (26.63 KiB) Viewed 36 times

: Given The Accompanying Gc Ms Data Pgs 8 10 26 Is The Crude Product A B Ready For Re Distillation A Or Should It 3 (25.25 KiB) Viewed 36 times

: Given The Accompanying Gc Ms Data Pgs 8 10 26 Is The Crude Product A B Ready For Re Distillation A Or Should It 4 (24.54 KiB) Viewed 36 times

Given the accompanying GC/MS data (pgs. 8-10) 26. Is the crude product A, B, ready for re-distillation (a) or should it be reworked to complete the reaction more (b)? a. Redistill b. Rework the reaction, then redistill. 27. Is the redistilled product OK to ship to the customer (a), or does it need to be reworked (a)? a. Redistill b. Rework the reaction, then redistill.
A File Operator 1 Acquired : 27 Jun 2019 12:44 pm using AcqMethod SPLITLESSGas.M Instrument 1 Instrument Sample Name: Misc Info : + Cyclohexanol Crude product peak I :C:\madchen\1\data\INSTRUMENT 1008.0 GC MS Number: 1 Abundance 1.26+07 1.16.07 16.07 9000000 8000000 7000000 5000000 5000000 4000000 3000000 2000000 1000000 Time-> Abundance 2200000 2000000 1800000 1000000 1400000 1200000 1000000 800000 600000 400000 200000 miz- 4.00 6.00 8.00 cyclohexene 35 39.2 10.00 40 45 48.1 12.00 14.00 16.00 18.00 20.00 22.00 Scan 127 (3.828 min): INSTRUMENT 1,008 Didata ms 51.2 50 TIC: INSTRUMENT 1 008 Didame 54.2 55 * Cyclohexene 57.2 60.1 63.1 65 74.1 75 79.2 80 24.00 86.0 26.00 28.00 95 100
File Operater 1 Acquired 27 Jun 2019 12:44 pm using Acethod SPLITLESSGAN.M Instrumenti Instrument 1 Sample Name: Mise into 1 Mumber: 1 6C MS Abundance 12-07 1.10-07 le+07 0000000 8000000 7000000 8000000 5000000 4000000 3000000 2000000 1000000 Abundance 2400000 000000 1600000 1400000 1200000 1000000 000000 000000 400000 200000 12- Cyclohexanol Cyclohexene Crude Product Peak 2 C:\madchen\\data\INSTRUMENT 1,000.0 4.00 Page 9 6.00 442 8.00 10.00 12:00 14.00 57.2 472 TO INSTRUMENT cyclohexanol 95.1 18:00 18.00 INSTRUMENT 008 100.2 100 110 120 8 9 20.00 22.00 34.00 26.00 180 20.00 2072 100 200 210
Re-Distilled Product File Operator Acquired Instrument: Sample Name: Mise Info GC MS : Mumber: 1 Abuntense 7000000 6000000 5000000 4000000 3000000 2000000 1000000 Time Abundance 2200000 2000000 1000000 1600000 1400000 1200000 1000000 800000 800000 C:\madchem\1\data\INSTRUMENT 1.007.0 : 27 Jun 2019 12:03 pm using Acqethod SPLITLESSGAS.M Instrument 1 400000 200000 4.00 6.00 8.00 10.00 cyclohexene 36.1 Page 10 30.2 40 Cyclohexanol Cyclohexene 42.2 48.1 TIC INSTRUMENT 1007 Didam 12.00 14.00 16.00 18:00 20.00 22:00 Sean 127 (3.828 min: INSTRUMENT 1008 Didalaine 50 54.2 66 572 801 00 63.1 45 67.2 70 74.1 80 24.00 26.00 860 91.1 85 90 96 28.00 100