Answer Happy

Posted: **Sun Jul 10, 2022 3:48 pm**

: Given The Accompanying Gc Ms Data Pgs 8 10 26 Is The Crude Product A B Ready For Re Distillation A Or Should It 1 (20.44 KiB) Viewed 32 times

: Given The Accompanying Gc Ms Data Pgs 8 10 26 Is The Crude Product A B Ready For Re Distillation A Or Should It 2 (34.92 KiB) Viewed 32 times

: Given The Accompanying Gc Ms Data Pgs 8 10 26 Is The Crude Product A B Ready For Re Distillation A Or Should It 3 (35.51 KiB) Viewed 32 times

: Given The Accompanying Gc Ms Data Pgs 8 10 26 Is The Crude Product A B Ready For Re Distillation A Or Should It 4 (34.01 KiB) Viewed 32 times

Given the accompanying GC/MS data (pgs. 8-10) 26. Is the crude product A, B, ready for re-distillation (a) or should it be reworked to complete the reaction more (b)? a. Redistill b. Rework the reaction, then redistill. 27. Is the redistilled product OK to ship to the customer (a), or does it need to be reworked (a)? a. Redistill b. Rework the reaction, then redistill.
Cyclohexanol Cyclohexene A Crude product peak I Cr\madchen\1\data\INSTRUMENT 100.00 File Operator Acquired Instrument Sample Nase Mise Info GC MS Abundance Humbert I 1.2007 13.07 16+07 000000 000000 7000000 000000 5000000 000000 3000000 2000000 1000000 Time Abundance 2200000 2000000 100000 1400000 1200000 1000000 800000 000000 400000 21 Jun 2019 12:44 pe using AcqMethod SPLITLESSGAS.M Instrument 1 200000 4.00 Рада 8 6.00 8.00 10.00 cyclohexene 422 20.00 14.00 12:00 16:00 Scan 127 82 mir INSTRUMENT 1006.data. 51.2 TIC: INSTRUMENT 1000 D 50 542 522 601 16 63.1 16:00 472 R 341 762 NO 24,00 25.00 100
B File Operator Acquired Instrument Sample Name: Miso Into 1 boc MS Abundance Number: 1 1.10-07 le-07 0000000 000000 7000000 000000 5000000 4000000 3000000 2000000 1000000 Time Abundance 2400000 200000 2000000 1000000 1000000 1400000 1200000 1000000 500000 500000 Cyclohexanol Cyclohexene Crude Product Peak 2 C:\nadchen\1\data\INSTRUMENT 1008.01 400000 200000 27 Jun 2019 12:44 pm using Acqethod SPLITLESSOAS M Instrument 1 4,00 362 Page 9 6.00 50 8.00 57.2 672 8 10.00 60 70 82.2 00 12.00 14.00 16.00 18.00 20.00 22:00 Scan 686 (7.112 min) INSTRUMENT 1 008.Didatams cyclohexanol TIC INSTRUMENT 1008 911 90 1002 100 110 120 130 100 150 140 24.00 170 180 25.00 100 20.00 200 2012 210
Re-Distilled Product File. Operator Acquired Instrument Sample Name: Mise Info 60 MS Nbundec 8000000 7000000 000000 5000000 000000 3000000 2000000 1000000 Abundance 2200000 2000000 1000000 10000 1400000 1200000 1000000 000000 600000 400000 200000 C\madchen\1\data\INSTRUMENT 1007.0 21 Jun 2019 12:03 pm using Acqethod SPLITLESSG. Instrument 1 4,00 6:00 8.00 cyclohexene Page 10 Cyclohexanol Cyclohexene 10.00 422 12.00 14.00 16.00 18.00 Sean 127 806 min) INSTRUMENT 1 008 67.2 48.1 $1.2 TIC INSTRUMENT 1007 50 54.2 55 572 601 43.1 70 20.00 741 22.00 24.00 20.00 79.2 10 MO I 1