identify the unkown based on GCMS,IR AND H AND C NMR spectrum and explain why
Posted: Tue May 17, 2022 10:19 am
identify the unkown based on GCMS,IR AND H AND C NMR spectrum
and explain why
Unknown 39 Component A FTIR (ATR) 100 95 90 85 80 75 2558 70 2734 65 -3033 20562 60 55 50 %Transmittance -1336 45 40 891 839 35 -1186_1227 -751 cm-1 %Tcm-1 %T 604 36 1407 30 676 22 145468 699 13 149964 751 34 1603 76 839 43 1690 12 891 42 1952 88 924 43 2558 75 1030 68 2652 73 1074 64 2734 73 1186 39 2922 68 1227 33 2956 69 1290 72 3033 66 1336 52 3064 68 30 ZOP 25 20 -676 15 10 5 5 0 041 4000 3000 2000 1000 Wavenumber (cm-1)
Unknown 39 Component A 13C NMR 75 MHz CDCI; 41.1 DEPT 75 MHz CDCI: 150 50 100 ppm 220 210 200 190 180 170 160 150 140 130 120 90 80 110 100 ppm 70 60 50 40 30 20 10 0 -10
Unknown 39 Component A 1H NMR 300 MHz CDC13 위 NNN 9 —10.69 14 12 10 8 ppm 7.5 7.4 7.2 7.1 7.3 ppm 14.0 13.5 13.0 12.5 12.0 11.5 11.0 10.5 10.0 9.5 9.0 8.5 8.0 7.5 7.0 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 6.5 ppm 0.0 -0.5
and explain why
- Identify The Unkown Based On Gcms Ir And H And C Nmr Spectrum And Explain Why 1 (112.32 KiB) Viewed 81 times
Unknown 39 Component A 13C NMR 75 MHz CDCI; 41.1 DEPT 75 MHz CDCI: 150 50 100 ppm 220 210 200 190 180 170 160 150 140 130 120 90 80 110 100 ppm 70 60 50 40 30 20 10 0 -10
Unknown 39 Component A 1H NMR 300 MHz CDC13 위 NNN 9 —10.69 14 12 10 8 ppm 7.5 7.4 7.2 7.1 7.3 ppm 14.0 13.5 13.0 12.5 12.0 11.5 11.0 10.5 10.0 9.5 9.0 8.5 8.0 7.5 7.0 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 6.5 ppm 0.0 -0.5