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Sample Name: benzaldehydac Data Collected on: DD2-500-S500 Archive directory /home/tlslab/mrsys/data/tislab Sample directory! benzaldehydec_20140425.01 FidFile: CARBON_01 ; 900 128.365 128.023 77.255 4.76.747 50.741 ----40,876 -32.179 31.822 29.250 27.322 Pulse Sequencer CARBON (s2pul) Solvent: adel3 Data collected on: Apr 25 2014 Temp. 25.0 C / 298.1 K Sample 49, Operator tlslab -126.346 Relax. delay 1.000 sec Pulse 45.0 degrees Acc. time 1.049 sec width 31250.0 Hz 256 repetitions OBSERVE 013, 125.6720314 M DECOUPIE 1, 499.7914486 ME Power 45 as continuously on WALTZ-16 modulated DATA PROCESSING Line broadening 0.5 2 IT size 65536 os Total time min 44 sec -115.676 -146.073 220 200 180 160 140 120 100 80 60 40 20 0 ppm

Bonzaldehyde derivative of Xantha nedione Archive directory: /export/home/TVO1ab/vnnr sys/data Sample directory: CMNP 248_21 Apr 2004 Pulse Sequence: s2pu 1 Solvent: COC13 Temp. 18.0 C / 291.1 K F118: PROTON INOVA-500 NMR500" Relax. delay 1.000 sec Pulse 45.0 degrees ACQ. tine 1.852 sec Vidth 7990.0 Hz 3 repetitions OBSERVEHI, 499.73B3644 MHZ DATA PROCESSING FT size 32768 Total tine Orin, 29 sec ppm 4.50 6.7.62 2.23 1.07 2.12 4.58 1.00