1.0 0.8 0.6 Transmitance Tamm 0.4 0.2 0.0 4000 3500 3000 2500 2000 1500 1000 500 Wavenumbers (cm-1)
Posted: Mon May 02, 2022 8:05 pm
- 1 0 0 8 0 6 Transmitance Tamm 0 4 0 2 0 0 4000 3500 3000 2500 2000 1500 1000 500 Wavenumbers Cm 1 1 (109.64 KiB) Viewed 48 times
Standard retention time of dichloromethane:2.26 min
Standard retention time of cyclohexanol:9.58 min
Standard retention time of cyclohexene:4.35 min
Product
Retention time of your product:4.51 min
Area for your product peak:3.01 cm2
Retention time of any remaining starting alcohol:9.52 min
Area for your starting alcohol: 0.51 cm2
Analysis of Reaction Mixture
Percent composition of alkene product (%) 85.51%
Percent composition of alcohol starting material (%) 14.49%
Based on GC data, calculate the actual mass of product obtained
(g) 9.18g
Actual product percent yield (%) 78.16%
2. Use 1-2 key peaks to justify what compound(s) that
you think are present.
3. Does this suggest that your reaction worked? Use 1 or
two key IR peaks to justify your answer.
4. What does this IR data indicate about the purity of
the product? Use 1 or two key IR peaks to justify your
answer.
1.0 0.8 0.6 Transmitance Tamm 0.4 0.2 0.0 4000 3500 3000 2500 2000 1500 1000 500 Wavenumbers (cm-1)